HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17800145, compound → HCID 23292346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17800145 | HCID 17800145 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23292346 | HCID 23292346 | — |
Reaction Steps
A suspension of 0.52 g (1.62 mmol) of the compound obtained in Step 2 (diastereoisomer 1) and of 0.1 g of Pd/Al2O3 in 60 ml of EtOH is hydrogenated at 20° C. under 1 bar for 16 hours. The mixture is then filtered and concentrated in vacuo to yield the title compound in the form of a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127396 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-2db60753db0c41bab30c4b94994d9d5d |
| Source note | uspto-grants-2000_10 |