N,N,N',N'-Tetramethylmethanediamine → HCID 10856106, compound

HRID 365934Notes

Reaction equation

HRID 365934 reaction equation
[CH2:1]([C:5]1[NH:6][CH:7]=[CH:8][N:9]=1)[CH2:2][CH2:3][CH3:4].[CH3:10][N:11]([CH2:13]N(C)C)[CH3:12]>O1CCCC1>[CH2:1]([C:5]1[N:9]([CH2:10][N:11]([CH3:13])[CH3:12])[CH:8]=[CH:7][N:6]=1)[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 5829N,N,N',N'-TetramethylmethanediamineHCID 118153512-butyl-1H-imidazole

Product 1

HCID 10856106HCID 10856106, compoundYield 103%

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

12.4 g of butylimidazole and 20.4 g of bis-(dimethylamino)methane were refluxed in 100 ml of tetrahydrofuran for 24 hours. The solvent was evaporated to give 18.64 g of product. The yield was quantitative. Other data concerning the product was:

Workup

  1. customThe solvent was evaporated

Sources & evidence

ORD record
ord-1ede9acf1361443b8322763d2323ae78
Source dataset
uspto-grants-2000_10
Patent number
US06127548

Reaction notes

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