HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131722053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131722055 | HCID 131722055 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131722053 | HCID 131722053 | — |
Reaction Steps
Prepared according to the method described in Example 1(e) above from (R)-N5 -(Cbz)-N2 -(diphenylacetyl)-N-(1-methyl-1-phenylethyl)ornithine amide (4.21 g; from step (c) above) using 10% Pd/C (200 mg) in 150 mL of MeOH and 1 mL of concentrated HCl, yielding 3.88 g of sub-title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06127414 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-128889dda2524278b837b7c8215e18bf |
| Source note | uspto-grants-2000_10 |