HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → 6,7-Dihydro-5h-benzo[6,7]cyclohepta[1,2-b]quinolin-8-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | Benzosuberone | HCID 70003 | — |
| Reactant | 2-Aminobenzonitrile | HCID 72913 | — |
| Product | 6,7-Dihydro-5h-benzo[6,7]cyclohepta[1,2-b]quinolin-8-amine | HCID 402666 | — |
Reaction Steps
2-amino-1-cyano-benzene (2.0 g, 16.9 mmol), 1-benzosuberone (6, 7, 8, 9-tetrahydrobenzocyclohepten-5-one) (3.0 g, 18.7 mmol) and boron trifluoride diethyl etherate(1M, 2.6 ml, 18.7 mmol) were treated according to the general procedure described herein to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130228 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-d1c7110dad284227a64f47d1282aca0a |
| Source note | uspto-grants-2000_10 |