HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[5-(3-Methoxyphenyl)-1,2,4-oxadiazol-3-yl]pyridine → HCID 23289232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[5-(3-Methoxyphenyl)-1,2,4-oxadiazol-3-yl]pyridine | HCID 789858 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23289232 | HCID 23289232 | — |
Reaction Steps
3-[5-(3-Methoxyphenyl)-[1,2,4]oxadiazol-3-yl)pyridine (4.0 g, 15.79 mM) and pyridine hydrochloride (37.6 g, 325 mM) were melted together at about 160° C. under an atmosphere of nitrogen for about 30 hours. This mixture was poured into H2O and stirred. The precipitated product was filtered and dried, 2.9 g, mp. >200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130217 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-5f31d29052804a36bc3c0b6fae16b13b |
| Source note | uspto-grants-2000_10 |