Dimethyl Ether → HCID 23289354, compound

HRID 366468Notes

Reaction equation

[Cl:1][C:2]1[C:7]2[N:8]=[C:9]([CH3:11])[S:10][C:6]=2[C:5]([O:12]C)=[CH:4][CH:3]=1.COC.Cl.N1C=CC=CC=1>>[Cl:1][C:2]1[C:7]2[N:8]=[C:9]([CH3:11])[S:10][C:6]=2[C:5]([OH:12])=[CH:4][CH:3]=1

Participants

Reactant 3

HCID 8254Dimethyl Ether

HCID 10176127Pyridinium chloride

HCID 23289310HCID 23289310, compound

Product 1

HCID 23289354HCID 23289354, compound

Procedure

The title compound was prepared from 4-chloro-7-methoxy-2-methylbenzothiazole by cleavage of the methyl ether with pyridine hydrochloride as described in Preparation 1, m.p. 225° C. (decomposition), mass spec. m/z 200.

Workup

customas described in Preparation 1, m.p. 225° C. (decomposition), mass spec

Sources & evidence

ORD record: ord-d00efb62822042d3bc8610f03fa7c165
Source dataset: uspto-grants-2000_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06130217

Reaction notes

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