HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Ether → 4-Chloro-2-methyl-1,3-benzothiazol-7-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Ether | HCID 8254 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 23289310 | HCID 23289310 | — |
| Product | 4-Chloro-2-methyl-1,3-benzothiazol-7-ol | HCID 23289354 | — |
Reaction Steps
The title compound was prepared from 4-chloro-7-methoxy-2-methylbenzothiazole by cleavage of the methyl ether with pyridine hydrochloride as described in Preparation 1, m.p. 225° C. (decomposition), mass spec. m/z 200.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130217 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-d00efb62822042d3bc8610f03fa7c165 |
| Source note | uspto-grants-2000_10 |