反应详情

温度

180 °C

A mixture of n-octylamine (24.2 g) and 3-oxabicyclo[3.1.0]hexane-2,4-dione (20.0 g) was heated at 180° C. for 2.5 hours and was then cooled to room temperature. The mixture was distilled in vacuo (boiling point 140-142° C. @ 0.1 mmHg) to give the title compound as a colourless oil.

1. temperaturewas then cooled to room temperature
2. distillationThe mixture was distilled in vacuo (boiling point 140-142° C. @ 0.1 mmHg)