참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Octylamine | HCID 8143 | — |
| 반응물 | 3-Oxabicyclo(3.1.0)hexane-2,4-dione | HCID 2734721 | — |
| 생성물 | 3-Octyl-3-azabicyclo[3.1.0]hexane-2,4-dione | HCID 3796377 | — |
반응 단계
A mixture of n-octylamine (24.2 g) and 3-oxabicyclo[3.1.0]hexane-2,4-dione (20.0 g) was heated at 180° C. for 2.5 hours and was then cooled to room temperature. The mixture was distilled in vacuo (boiling point 140-142° C. @ 0.1 mmHg) to give the title compound as a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06130241 |
|---|
| 출처 데이터셋 | uspto-grants-2000_10 |
|---|
| ORD ID | ord-205c7744a0ef44b9b38d77991e183f5b |
|---|
| 출처 메모 | uspto-grants-2000_10 |
|---|
