HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → 1-(4-Chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | 2-((4-Chlorophenoxy)methyl)oxirane | HCID 91515 | — |
| Reactant | 2-Methoxyethyl benzoate | HCID 228741 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | 1-(4-Chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate | HCID 9950980 | 93% |
Reaction Steps
A reaction was conducted as described in Example 6 except that benzoic acid was replaced with the same molar amount of 2-methoxyethyl benzoate, a compound represented by formula (3) where R2 is phenyl and OZ1 is an organic group derived from 2-methoxyethanol, and PGE was replaced with the same molar amount of 4-chlorophenyl glycidyl ether. Desired 1-(4-chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate was formed in an analytical yield of 93% and isolated in a yield of 86%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130346 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-ebe83e5750364f8bb5beeb9a960eb2ae |
| Source note | uspto-grants-2000_10 |