HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → HCID 9884634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | 4-Chlorophenyl 2-methylprop-2-enoate | HCID 12400851 | — |
| Product | HCID 9884634 | HCID 9884634 | 96% |
Reaction Steps
A reaction was conducted as described in Example 6 except that benzoic acid was replaced with the same molar amount of 4-chlorophenyl methacrylate, a compound represented by formula (3) where R2 is isopropenyl and OZ1 is an organic group derived from 4-chlorophenol. Desired 1-(4-chlorophenoxy)-3-phenoxy-2-propyl methacrylate was formed in an analytical yield of 96% and isolated in a yield of 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130346 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-9ecd4b4702e24ace818b439cba42de76 |
| Source note | uspto-grants-2000_10 |