Calcium Hydroxide → HCID 86755942, compound

HRID 366991Notes

Reaction equation

HRID 366991 reaction equation
[OH-].[Ca+2:2].[OH-].[Cl:4][C:5]1[CH:34]=[CH:33][C:8]([O:9][CH:10]([CH3:32])[CH2:11][O:12][N:13]=[C:14]([CH:18]2[C:23](=[O:24])[CH2:22][CH:21]([CH:25]3[CH2:30][CH2:29][CH2:28][S:27][CH2:26]3)[CH2:20][C:19]2=[O:31])[CH2:15][CH2:16][CH3:17])=[CH:7][CH:6]=1>CO>[Ca:2].[Cl:4][C:5]1[CH:34]=[CH:33][C:8]([O:9][CH:10]([CH3:32])[CH2:11][O:12][N:13]=[C:14]([CH:18]2[C:23](=[O:24])[CH2:22][CH:21]([CH:25]3[CH2:30][CH2:29][CH2:28][S:27][CH2:26]3)[CH2:20][C:19]2=[O:31])[CH2:15][CH2:16][CH3:17])=[CH:7][CH:6]=1

Participants

4

Reactant 2

HCID 6093208Calcium HydroxideHCID 54366352HCID 54366352, compound

Product 1

HCID 86755942HCID 86755942, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

A suspension of calcium hydroxide (0.2 g) in 30 ml of methanol was added to a solution of 2-{1-[2-(4-chlorophenoxy)propyloximino]butyl}-5-tetrahydrothiopyran-3-ylcyclohexane-1,3-dione (2.5 g) in 80 ml of methanol with vigorous stirring. The mixture was subsequently stirred for 5 hours at room temperature, whereupon the solvent was removed in vacuo. Yield: 2.6 g of calcium salt.

Workup

  1. customwas removed in vacuo

Sources & evidence

ORD record
ord-e1ef4ca0a13945dfb7ed1455a4da72de
Source dataset
uspto-grants-2000_10
Patent number
US06133202

Reaction notes

Loading…