Calcium Hydroxide → HCID 86755942, compound

Participants

Reaction Steps

A suspension of calcium hydroxide (0.2 g) in 30 ml of methanol was added to a solution of 2-{1-[2-(4-chlorophenoxy)propyloximino]butyl}-5-tetrahydrothiopyran-3-ylcyclohexane-1,3-dione (2.5 g) in 80 ml of methanol with vigorous stirring. The mixture was subsequently stirred for 5 hours at room temperature, whereupon the solvent was removed in vacuo. Yield: 2.6 g of calcium salt.

Provenance & Evidence