Cesium carbonate → HCID 23287555, compound

Participants

Reaction Steps

1-[2-(4-nitro-2,6-dimethoxyphenoxy)ethyl]pyrrolidine was prepared from 4-nitro-2,6-dimethoxyphenol [R F Collins and M Davis, J. Chem. Soc. 1863, (1961)] (0.4 g, 2.39 mmol), 1-(2-chloroethyl)pyrrolidine (612 mg, 0.36 mmol) and caesium carbonate (2.3 g, 0.72 mmol) to give the desired product as a brown oil (232 mg). MS (ES+) 297 (MH+).

Provenance & Evidence