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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 367144Generated: October 29, 2026

Methyl iodide → HCID 12216083, compound

https://huagongshe.com/reaction/367144

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantLithium hydrideHCID 62714—
Reactant4H-Pyrido[3,2-e]-1,3-thiazin-4-one, 2-(phenylamino)-HCID 12216078—
ProductHCID 12216083HCID 12216083—

Reaction Steps

The reaction procedure of Example 11 was followed except that 255 mg of 2-anilino-4H-pyrido[3,2-e]-1,3-thiazin-4-one, 9 mg of lithium hydride and 0.063 ml of methyl iodide were used. As a result, 113 mg of 3-methyl-2-phenylimino-2,3-dihydro-4H-pyrido[3,2-e]-1,3-thiazin-4-one was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06133258
Source datasetuspto-grants-2000_10
ORD IDord-285b4f74afa04553a1a9c82032de3d2f
Source noteuspto-grants-2000_10