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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 367155Generated: October 29, 2026

Methyl iodide → HCID 23287687, compound

https://huagongshe.com/reaction/367155

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantLithium hydrideHCID 62714—
ReactantHCID 1259240HCID 1259240—
ProductHCID 23287687HCID 23287687—

Reaction Steps

The reaction procedure of Example 11 was followed except that 1.31 g of ethyl 4-[(4-oxo-4H-pyrido[3,2-e]-1,3-thiazin-2-yl)amino]benzoate, 36 mg of lithium hydride and 0.25 ml of methyl iodide were used. As a result, 656 mg of ethyl 4-[(3-methyl-4-oxo-2,3-dihydro-4H-pyrido[3,2-e]-1,3-thiazin-2-ylidene)amino]benzoate was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06133258
Source datasetuspto-grants-2000_10
ORD IDord-bd06dbe90c234fe29966671a459b648b
Source noteuspto-grants-2000_10