HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium thiocyanate → HCID 57147179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium thiocyanate | HCID 15666 | — |
| Reactant | 2-Chloronicotinoyl chloride | HCID 2774541 | — |
| Reactant | Ethyl 4-(propylamino)benzoate | HCID 13314418 | — |
| Product | HCID 57147179 | HCID 57147179 | 86.9% |
Reaction Steps
The reaction procedure of Example 57 was followed except that 230 mg of 2-chloronicotinoyl chloride, 100 mg of ammonium thiocyanate and 270 mg of ethyl 4-(propylamino)benzoate were used. As a result, 418 mg of ethyl 4-[N-(4-oxo-4H-pyrido[3,2-e]-1,3-thiazin-2-yl)-N-propylamino)benzoate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133258 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-9c852386db7549e9994339038016abe7 |
| Source note | uspto-grants-2000_10 |