Ammonium thiocyanate → HCID 15485513, compound

Participants

Reaction Steps

The reaction procedure of Example 102 was followed except that 336 mg g of 2-chloronicotinoyl chloride, 145 mg of ammonium thiocyanate, 300 mg of 2-(methylamino)naphthalene and 7 ml of acetone were used. The product was then recrystallized from a mixture of ethanol and chloroform to obtain 321 mg of 2-[N-methyl-N-(2-naphthyl)amino]-4H-pyrido[3,2-e]-1,3-thiazin-4-one.

Provenance & Evidence