Ammonium thiocyanate → HCID 15485514, compound

Participants

Reaction Steps

The reaction procedure of Example 102 was followed except that 1.669 g of 2-chloronicotinoyl chloride, 722 mg of ammonium thiocyanate, 1.55 g of 5-(methylamino)benzo[b]thiophene and 35 ml of acetone were used. The product was then recrystallized from a mixture of ethanol and ethyl acetate to obtain 546 mg of 2-[N-(benzo[b]thiophen-5-yl)-N-methylamino]-4H-pyrido[3,2-e]-1,3-thiazin-4-one.

Provenance & Evidence