HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloroindole → HCID 9903606, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloroindole | HCID 87110 | — |
| Reactant | Octahydroindolizin-7-one | HCID 11240524 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 9903606 | HCID 9903606 | — |
Reaction Steps
5-Chloro-1H-indole (1.00 g, 6.63 mmol) and 7-octahydroindolizinone (1.39 g, 9.95 mmol) were converted to product by the procedure of Preparation 4 to give 595 mg. (33.1%). EA calculated for C16H17N2Cl: C, 70.45; H, 6.28; N, 10.27. Found: C, 70.60; H, 6.46; N, 10.28.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133290 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-c7ef9a3c32c54135896fe101ca7664b2 |
| Source note | uspto-grants-2000_10 |