HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromobenzenesulfonyl chloride → HCID 23288113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromobenzenesulfonyl chloride | HCID 520403 | — |
| Reactant | 5-fluoro-3-(1-methyl-1,2,3,6-tetrahydro-4-pyridinyl)-1H-indole | HCID 14973209 | — |
| Product | HCID 23288113 | HCID 23288113 | — |
Reaction Steps
(32 mg, 53%), from 5-fluoro-3-(1-methyl-1,2,3,6-tetrahydro-4-pyridinyl)-1H-indole (Example 4b, 30.6 mg, 0.133 mmol) and 2-bromophenylsulfonyl chloride (67.9 mg, 0.27 mmol); HRMS-FAB+ for C20H19N2SO2BrF calculated MH+ : 449.03348; found: 449.03240.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133287 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-f2ef83e685884817ba26a81a76ec17f1 |
| Source note | uspto-grants-2000_10 |