HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzenesulfonyl chloride → HCID 23288128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzenesulfonyl chloride | HCID 9588 | — |
| Reactant | 5-Chloro-3-(1-methyl-4-piperidinyl)indole | HCID 11413992 | — |
| Reactant | HCID 23288115 | HCID 23288115 | — |
| Product | HCID 23288128 | HCID 23288128 | — |
Reaction Steps
(ttt) 5-Chloro-1-(4-fluorophenylsulfonyl )-3-(1-methyl-4-piperidinyl)indole (18.4 mg, 45%) from 5-chloro-3-(1-methyl-4-piperidinyl)-1H-indole (Example 5e, 25 mg, 0.1 mmol) and 4-fluorophenylsulfonyl chloride (29.2 mg, 0.15 mmol), HRMS-FAB+ for C20H20N2O2SClF, calculated MH+ : 407.09964; found: 407.09685.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133287 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-8dcd82a8c806422083faf300798b8b42 |
| Source note | uspto-grants-2000_10 |