HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzenesulfonyl chloride → HCID 23288138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzenesulfonyl chloride | HCID 9588 | — |
| Reactant | 1H-Indole, 6-chloro-3-(1-methyl-4-piperidinyl)- | HCID 18797368 | — |
| Reactant | HCID 23288102 | HCID 23288102 | — |
| Product | HCID 23288138 | HCID 23288138 | — |
Reaction Steps
1-(4-Fluorophenylsulfonyl)-6-chloro-3-(1-methyl-4-piperidinyl)indole: (26.8 mg, 65%), from 6-chloro-3-(1-methyl-4-piperidinyl)-1H-indole (Example 5b, 25 mg, 0.10 mmol) and 4-fluorophenylsulfonyl chloride (29.2 mg, 0.15 mmol), HRMS-FAB+ for C20H20N2O2SClF, calculated MH+ : 407.09964; found: 407.09929.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133287 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-1636e22e03a84594b4c2f8a961763e76 |
| Source note | uspto-grants-2000_10 |