HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178450981, compound → HCID 178450988, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178450981 | HCID 178450981 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178450988 | HCID 178450988 | 98.4% |
Reaction Steps
In 100 ml of methanol was dissolved 3.73 g of N-benzyloxycarbonyl-L-leucyl-L-argininal dibutyl acetal obtained. In nitrogen atmosphere, 1 g of palladium black was added to the solution and the mixture was subjected to catalytic hydrogenation at room temperature for 2 hours. After palladium black was removed by filtration, the filtrate was concentrated under reduced pressure to give 2.75 g of L-leucyl-L-argininal dibutyl acetal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05416238 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-18dbffb3ffe24dd28162ca1f1a413a29 |
| Source note | uspto-grants-1995_05 |