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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 36805Generated: October 26, 2026

HCID 178450981, compound → HCID 178450988, compound

https://huagongshe.com/reaction/36805

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178450981HCID 178450981—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 178450988HCID 17845098898.4%

Reaction Steps

In 100 ml of methanol was dissolved 3.73 g of N-benzyloxycarbonyl-L-leucyl-L-argininal dibutyl acetal obtained. In nitrogen atmosphere, 1 g of palladium black was added to the solution and the mixture was subjected to catalytic hydrogenation at room temperature for 2 hours. After palladium black was removed by filtration, the filtrate was concentrated under reduced pressure to give 2.75 g of L-leucyl-L-argininal dibutyl acetal.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05416238
Source datasetuspto-grants-1995_05
ORD IDord-18dbffb3ffe24dd28162ca1f1a413a29
Source noteuspto-grants-1995_05