Cyclohexyl isocyanate → HCID 15485708, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of cyclohexyl isocyanate (400 mg, 3.19 mmol) in toluene, 2-amino-5-nitrophenol (492 mg, 3.19 mmol) was added. The reaction mixture was stirred at 80° C. for 24 hours, then cooled to room temperature. The product was purified by precipitation from toluene and filtering (752 mg, 93%). m.p: 1850-186.0° C.; EI-MS m/z 280 (M+H)+.

Provenance & Evidence