Isopropyl isocyanate → HCID 23288441, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of isopropyl isocyanate (221 mg, 2.6 mmol) in toluene, 2-amino-5-nitrophenol (400 mg, 2.6 mmol) was added. The reaction mixture was stirred at 80° C. for 24 hours, then cooled to room temperature. The product was purified by precipitation from toluene and filtering (570 mg, 92%). m.p: 159.8-161.4° C.; EI-MS m/z 240 (M+H)+.

Provenance & Evidence