Isopropyl isocyanate → HCID 23288444, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of isopropylisocyanate (31.2 mg, 0.37 mmol) in DMF (0.5 ml), 2-benzenesulfonylamino-4-cyanoaniline (100 mg, 0.37 mmol) was added. The reaction mixture was stirred at 80° C. for 3 hours. Chromatography of the resulting liquid on silica gel gave the desired product (85 mg, 65%). EI-MS m/z 359.4 (M+).

Provenance & Evidence