HRID368468

反应详情

EQUATION

反应方程式

HRID 368468 的结构方程式

PROCEDURE

实验过程

To 800 mg of trifluoroacetic acid was added 340 mg of 2-t-butylamino-3-fluoro-5-methyl-6-(1,1,3,3-tetramethylbutylamino)pyridine, and the mixture was allowed to stand at room temperature for 30 minutes. The solution was concentrated under reduced pressure to obtain crude 2,6-diamino-3-fluoro-5-methylpyridine as a pale brown solid residue.

WORKUP

后处理

  1. concentrationThe solution was concentrated under reduced pressure