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HRID368586

反应详情

EQUATION

反应方程式

HRID 368586 的结构方程式

REACTANTS

反应物

2
结构：C[Si](C)(Cl)CCl
HCID74393

Silane, chloro(chloromethyl)dimethyl-

C3H8Cl2Si

结构：CCN(CC)C(=O)c1ccccc1Cl
HCID82566

2-Chloro-N,N-diethylbenzamide

C11H14ClNO

PRODUCTS

生成物

1
结构：CCN(CC)C(=O)c1c(Cl)cccc1[Si](C)(C)CCl
HCID18630016

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to General Method A from the compound of Example e and 1.5 eq (chloromethyl)dimethylsilyl chloride. Purification by HPLC using 1:9 ethyl acetate/hexanes gave 5.4 g of the desired compound as a yellow oil, an 85% yield.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by HPLC