化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | N-Isopropylhydroxylamine Hydrochloride | HCID 170873 | — |
| 反応物 | 2-Chloro-6-(trimethylsilyl)benzoyl chloride | HCID 15183557 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | 2-Chloro-n-hydroxy-n-(1-methylethyl)-6-(trimethylsilyl)benzamide | HCID 18630150 | — |
反応手順
The title compound was prepared by reaction of the compound of Example b and the i-propylhydroxylamine hydrochloride in dioxane in the presence of two equivalents of triethylamine using the amination methods described above. m.p. 175-179° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06133252 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-58ede89b1a4445c48b4b5908b0f6f8c5 |
| 出典メモ | uspto-grants-2000_10 |