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HRID368618

反应详情

EQUATION

反应方程式

HRID 368618 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC(C)NO.Cl
HCID170873

N-Isopropyl hydroxylamine

C3H10ClNO

结构：C[Si](C)(C)c1cccc(Cl)c1C(=O)Cl
HCID15183557

2-Chloro-6-(trimethylsilyl)benzoyl chloride

C10H12Cl2OSi

PRODUCTS

生成物

1
结构：CC(C)N(O)C(=O)c1c(Cl)cccc1[Si](C)(C)C
HCID18630150

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

The title compound was prepared by reaction of the compound of Example b and the i-propylhydroxylamine hydrochloride in dioxane in the presence of two equivalents of triethylamine using the amination methods described above. m.p. 175-179° C.