HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → (4-Hydroxyphenyl)acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | 4-Hydroxybenzyl cyanide | HCID 26548 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | (4-Hydroxyphenyl)acetamide | HCID 86986 | 98,4% |
Reaktionsschritte
(0.0032 g, 0.007 mmol) of the platinum complex, prepared as in Example 1, was stirred with 4-hydroxybenzyl cyanide (1.0 g, 7.5 mmol) and 5 ml (0.28 mol) of water and 5 ml ethanol and the mixture heated under reflux for 18 hours. After cooling the liquids were removed using a rotary evaporator to give 4-hydroxy phenylacetamide (1.116 g) corresponding to 98% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133478 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-4d6952dc87e34863ae75f5dd9576b424 |
| Quellennotiz | uspto-grants-2000_10 |