HRID368810

反应详情

EQUATION

反应方程式

HRID 368810 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

(0.0032 g, 0.007 mmol) of the platinum complex, prepared as in Example 1, was stirred with 4-hydroxybenzyl cyanide (1.0 g, 7.5 mmol) and 5 ml (0.28 mol) of water and 5 ml ethanol and the mixture heated under reflux for 18 hours. After cooling the liquids were removed using a rotary evaporator to give 4-hydroxy phenylacetamide (1.116 g) corresponding to 98% yield.

WORKUP

后处理

  1. custom(0.0032 g, 0.007 mmol) of the platinum complex, prepared as in Example 1
  2. temperaturethe mixture heated
  3. temperatureunder reflux for 18 hours
  4. temperatureAfter cooling the liquids
  5. customwere removed
  6. customa rotary evaporator