HRID368810
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
(0.0032 g, 0.007 mmol) of the platinum complex, prepared as in Example 1, was stirred with 4-hydroxybenzyl cyanide (1.0 g, 7.5 mmol) and 5 ml (0.28 mol) of water and 5 ml ethanol and the mixture heated under reflux for 18 hours. After cooling the liquids were removed using a rotary evaporator to give 4-hydroxy phenylacetamide (1.116 g) corresponding to 98% yield.
WORKUP
后处理
- custom(0.0032 g, 0.007 mmol) of the platinum complex, prepared as in Example 1
- temperaturethe mixture heated
- temperatureunder reflux for 18 hours
- temperatureAfter cooling the liquids
- customwere removed
- customa rotary evaporator