HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23284422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 23284431 | HCID 23284431 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23284422 | HCID 23284422 | 68.6% |
Reaction Steps
) 3.18 g of N-(2-nitro-4-trifluoromethyl-5-fluorophenyl)-aminomethanephosphonic acid is stirred together with 3.18 g of sodium carbonate and 2.82 g of phenol in 40 ml of water for 4 hours at a bath temperature of 120° C. After acidification with 4N hydrochloric acid, the precipitated product is suctioned off. 2.69 g of N-(2-nitro-4-TRIFLUOROMETHYL-5-phenoxyphenyl)-aminomethanephosphonic acid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06136805 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-9536476cb1fb4cdc9d4a758d14eee5e8 |
| Source note | uspto-grants-2000_10 |