HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 23284869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 22004680 | HCID 22004680 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23284869 | HCID 23284869 | — |
Reaction Steps
Trifluoroacetic acid (10 ml) was added to a solution of N-{[1-(tert-butoxycarbonyl)-4-piperidyl]methyl}pyridine-2-sulphonamide (1.45 g) in dichloromethane (10 ml) and the mixture stirred at ambient temperature for 1.5 hours. The solvent was removed under reduced pressure to yield crude N-(4-piperidyl methyl)pyridine-2-sulphonamide trifluoroacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06136825 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-ad49eaa491e44d54b02c5b0ebbd921af |
| Source note | uspto-grants-2000_10 |