Methyl iodide → HCID 23285598, compound

HRID 369197Notes

Reaction equation

HRID 369197 reaction equation
[Cl:1][C:2]1[C:3]([CH2:11][CH:12]([CH2:17][N:18]([CH3:20])[CH3:19])[C:13]([O:15][CH3:16])=[O:14])=[CH:4][C:5]2[O:9][CH2:8][O:7][C:6]=2[CH:10]=1.[CH3:21][I:22]>C(O)(C)C>[I-:22].[Cl:1][C:2]1[C:3]([CH2:11][CH:12]([C:13]([O:15][CH3:16])=[O:14])[CH2:17][N+:18]([CH3:21])([CH3:19])[CH3:20])=[CH:4][C:5]2[O:9][CH2:8][O:7][C:6]=2[CH:10]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 23285600HCID 23285600, compound

Product 1

HCID 23285598HCID 23285598, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

The operation is carried out as in Stage 2 of Example 1, starting with 436 mg of the product obtained in Stage 2 above, 6 ml isopropanol and 0.27 ml of methyl iodide. In this way 501 mg of expected product is obtained.

Sources & evidence

ORD record
ord-2b2c518e3e7f46eb99b22ea39a617fc4
Source dataset
uspto-grants-2000_10
Patent number
US06136842

Reaction notes

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