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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 369550Generated: October 30, 2026

HCID 54451764, compound → HCID 53656749, compound

https://huagongshe.com/reaction/369550

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54451764HCID 54451764—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 53656749HCID 53656749100%

Reaction Steps

A small scoop of 10% Pd/C catalyst was added to a solution of 41c in 15 ml methanol. The flask was evacuated and filled with hydrogen three time. The reaction mixture was stirred three hours under H2 balloon atmosphere and filtered through a pad of celite. Evaporation of solvent yielded 169 mg (100%) of a gray solid. The crude product was used without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06139771
Source datasetuspto-grants-2000_10
ORD IDord-88149f1e6958474bbf0fc99605ea7ebf
Source noteuspto-grants-2000_10