HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Methylpyridin-2-yl)methanol → 2-Pyridinemethanol, 5-ethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Methylpyridin-2-yl)methanol | HCID 12325387 | — |
| Reactant | (5-Ethylpyridin-2-yl)methyl acetate | HCID 14346253 | — |
| Product | 2-Pyridinemethanol, 5-ethyl- | HCID 3013942 | 85% |
Reaction Steps
This synthesis was performed analogously to the synthesis reported for 2-hydroxymethyl-5-methyl pyridine. Starting from 2-acetoxymethyl-5-ethyl pyridine (40 g, 223 mmol), pure 2-hydroxymethyl-5-ethyl pyridine (26.02 g, 189 mmol, 85%) was obtained as a slightly yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06140294 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-1b1eecef0cee474b995a1b3ff7247057 |
| Source note | uspto-grants-2000_10 |