Hydrochloric Acid → HCID 18534817, compound

HRID 369827Notes

Reaction equation

HRID 369827 reaction equation
[CH3:1][C:2]1([CH3:11])[C:7](=[O:8])[O:6][CH2:5][C:4]([CH3:10])([CH3:9])[NH:3]1.Cl.[CH2:13]1[O:15][CH2:14]1>CO>[OH:15][CH2:14][CH2:13][N:3]1[C:4]([CH3:10])([CH3:9])[CH2:5][O:6][C:7](=[O:8])[C:2]1([CH3:11])[CH3:1]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 6354Ethylene OxideHCID 131312033,3,5,5-Tetramethylmorpholin-2-one

Product 1

HCID 18534817HCID 18534817, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

45.0 g (0.29 moles) of 3,3,5,5-tetramethyl-2-morpholone are dissolved in 450 ml of methanol. The solution is poured into an autoclave, added with 1 ml of concentrated HCl (37%) (% w/w) and pressurized with ethylene oxide (2 bars).

Workup

  1. additionThe solution is poured into an autoclave

Sources & evidence

ORD record
ord-1762112e52794ef2bb1405e1e80f6eb5
Source dataset
uspto-grants-2000_10
Patent number
US06140326

Reaction notes

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