HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-(2-Phenylethyl)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Propionyl chloride | HCID 62324 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(2-Phenylethyl)propanamide | HCID 94894 | — |
Reaction Steps
The title compound was prepared in a reaction between phenethylamine (12.1 g, 100 mmol), propionyl chloride (9.25 g, 100 mmol) and triethylamine (20 ml) in methylene chloride (200 ml). The product (10.1 g) was used without purification; MS [M+H]+ 178.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06140322 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-b43314afbe2b4d14917fc8f07abfcb33 |
| Source note | uspto-grants-2000_10 |