HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 70043658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-[2-Butyl-3-(2-nitro-benzyl)-3H-imidazol-4-yl]-2-thiophen-2-ylmethyl-acrylic acid | HCID 14952906 | — |
| Product | HCID 70043658 | HCID 70043658 | — |
Reaction Steps
(E)-3-[2-n-Butyl-1-{(2-nitrophenyl)methyl}-1H-imidazol-5-yl]-2-(2-thienyl)methyl-2-propenoic acid, prepared in Example 55, was treated with thionyl chloride and then ammonium hydroxide, as described in Example 54, to give the title compound; mp 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05418250 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-6a9b101bc495456d85ceb61efbcd487e |
| Source note | uspto-grants-1995_05 |