反应详情

A mixture of 6-aminohexan-1-ol (11.7 g, 10 mmol) and 1,2,4-benzenetricarboxylic anhydride (7.68 g, 4 mmol) was heated to 175°-225° C. for 15 min or until evolution of H2O vapor stops. The melt was poured into water to give a white crystalline solid. The solid was collected by vacuum filtration and dried overnight in vacuo to give 9.1 g (78%) of analytically pure 27.

1. customto give a white crystalline solid
2. filtrationThe solid was collected by vacuum filtration
3. customdried overnight in vacuo
4. customto give 9.1 g (78%) of analytically pure 27