O-Methylhydroxylamine hydrochloride → HCID 20275656, compound

HRID 370381Notes

Reaction equation

HRID 370381 reaction equation
[Cl:1][C:2]1[C:3]([O:12][C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-:21])=[O:20])=[C:15]([N+]([O-])=O)[CH:14]=2)=[N:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.Cl.[CH3:26][O:27][NH2:28]>>[N+:19]([C:16]1[CH:17]=[CH:18][C:13]([O:12][C:3]2[C:2]([Cl:1])=[CH:7][C:6]([C:8]([F:10])([F:11])[F:9])=[CH:5][N:4]=2)=[CH:14][C:15]=1[CH2:26][O:27][NH2:28])([O-:21])=[O:20]

Participants

3

Reactant 2

HCID 521874O-Methylhydroxylamine hydrochlorideHCID 202515733-Chloro-2-(3,4-dinitrophenoxy)-5-(trifluoromethyl)pyridine

Product 1

HCID 20275656HCID 20275656, compound

Procedure

Following the procedure of Example 29, 4-(3-chloro-5-trifluoromethyl-2-pyridyloxy)-1,2-dinitrobenzene and methoxyamine hydrochloride are reacted together to give N-[2-nitro-5-(3-chloro-5-trifluoromethyl-2-pyridyloxy)phenyl]methoxyamine (XV; R'=H). ##STR29##

Workup

  1. customare reacted together

Sources & evidence

ORD record
ord-56483cb7d9624d509e2543c24c24acfc
Source dataset
uspto-grants-1985_07
Patent number
US04526608

Reaction notes

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