HuagongsheHuagongshe Chemistry Print Report · For research reference only
Palmitoyl chloride → HCID 20275854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Palmitoyl chloride | HCID 8206 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dimedone | HCID 31358 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20275854 | HCID 20275854 | 67% |
Reaction Steps
Using the procedure described in Example III and starting with 3.00 g (0.0130 mol) of 2-4'-methylphenyl)-5,5-dimethyl-1,3-cyclohexanedione, 2.69 g (0.0098 mol) of palmitoyl chloride, 2.63 g (0.0260 mol) of triethylamine, and 30 ml of methylene chloride, 3.1 g (67% yield) of a clear, colorless oil was obtained as the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04526723 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-f2c4b8b3705f4e20b90c0f8058d290d2 |
| Source note | uspto-grants-1985_07 |