Hydroquinone → HCID 70477711, compound

HRID 370426Notes

Reaction equation

HRID 370426 reaction equation
[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2].C(Cl)(=[O:13])CCC>>[C:5]([OH:13])(=[O:6])[CH2:7][CH2:8][CH3:1].[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2]

Participants

3

Reactant 2

HCID 785HydroquinoneHCID 8855Butyryl chloride

Product 1

HCID 70477711HCID 70477711, compound

Procedure

According to the same procedure as described in Preparation 6, hydroquinone and butyryl chloride were reacted and the reaction mixture was extracted with ethyl acetate. The ethyl acetate extract was thoroughly washed with water and the solvent was removed. The residue was distilled under a reduced pressure to give hydroquinone monobutyrate. b.p. 150°-153° C./3 mmHg.

Workup

  1. customwere reacted
  2. extractionthe reaction mixture was extracted with ethyl acetate
  3. extractionThe ethyl acetate extract
  4. washwas thoroughly washed with water
  5. customthe solvent was removed
  6. distillationThe residue was distilled under a reduced pressure

Sources & evidence

ORD record
ord-a90dadbff19c4c1fbbab9053847c4692
Source dataset
uspto-grants-1985_07
Patent number
US04526779

Reaction notes

Loading…