HCID 13131603, compound → HCID 13131604, compound

HRID 370457Notes

Reaction equation

HRID 370457 reaction equation
C(OC([NH:8][N:9]1[CH2:17][C:16]2[C:11](=[C:12]([CH3:19])[CH:13]=[CH:14][C:15]=2[CH3:18])[CH2:10]1)=O)(C)(C)C>Cl>[NH2:8][N:9]1[CH2:10][C:11]2[C:16](=[C:15]([CH3:18])[CH:14]=[CH:13][C:12]=2[CH3:19])[CH2:17]1

Participants

3

Reactant 1

HCID 13131603HCID 13131603, compound

Product 1

HCID 13131604HCID 13131604, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

20 g of N-(t-butyloxycarbonylamino)-4,7-dimethylisoindoline are introduced into 200 ml of concentrated hydrochloric acid and stirred for 2 hours at room temperature. A yield of 17 g of the hydrochloride of 2-Amino-4,7-dimethylisoindoline precipitates in the form of crystals.

Workup

  1. customA yield of 17 g of the hydrochloride of 2-Amino-4,7-dimethylisoindoline precipitates in the form of crystals

Sources & evidence

ORD record
ord-34e298837b0d4d1e8dc40d01f270b3ec
Source dataset
uspto-grants-1985_07
Patent number
US04526897

Reaction notes

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