Sodium → HCID 178490926, compound

HRID 370530Notes

Reaction equation

HRID 370530 reaction equation
[CH3:1][O:2][C:3]1[CH:24]=[CH:23][C:6]([CH2:7][N:8]2[C:12]([S:13](C3C=CC(C)=CC=3)(=O)=O)=[N:11][N:10]=[N:9]2)=[CH:5][CH:4]=1.[Na]>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:7][N:8]2[C:12]([SH:13])=[N:11][N:10]=[N:9]2)=[CH:23][CH:24]=1

Participants

3

Reactant 2

HCID 5360545SodiumHCID 13518829HCID 13518829, compound

Product 1

HCID 178490926HCID 178490926, compound

Procedure

Treatment of the product of Example 4 as in the previous example gives the sodium salt of the title compound. This is recrystallized from ethyl acetate-hexane, m.p. 246°-250° C. (decomp).

Sources & evidence

ORD record
ord-325a0437b39f4e61a5402514c80b9031
Source dataset
uspto-grants-1985_07
Patent number
US04526978

Reaction notes

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