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HRID370647

反应详情

EQUATION

反应方程式

HRID 370647 的结构方程式

REACTANTS

反应物

3
结构：c1c[nH]cn1
HCID795

Imidazole

C3H4N2

结构：BrCCc1ccc2ccccc2c1
HCID228270

2-(2-bromoethyl)naphthalene

C12H11Br

结构：CC(C)(C)[O-].[K+]
HCID23665647

2-Methyl-2-propanol, potassium salt

C4H9KO

PRODUCTS

生成物

1
结构：c1ccc2cc(CCn3ccnc3)ccc2c1
HCID3058926

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCO
溶剂HCID263

1-Butanol

C4H10O

PROCEDURE

实验过程

A mixture of imidazole (1.02 g, 0.015 mol), 2-(2-bromoethyl)naphthalene (3.53 g, 0.015 mol) and potassium tert-butoxide (1.68 g, 0.015 mol) in dry butan-1-ol (100 ml) was stirred and heated under reflux for 29 h.

WORKUP

后处理

  1. temperatureheated
  2. temperatureunder reflux for 29 h.