HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → 1-[2-(2-Naphthyl)ethyl]imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | 2-(2-Bromoethyl)naphthalene | HCID 228270 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | 1-[2-(2-Naphthyl)ethyl]imidazole | HCID 3058926 | — |
Reaction Steps
A mixture of imidazole (1.02 g, 0.015 mol), 2-(2-bromoethyl)naphthalene (3.53 g, 0.015 mol) and potassium tert-butoxide (1.68 g, 0.015 mol) in dry butan-1-ol (100 ml) was stirred and heated under reflux for 29 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528195 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-072229e5e7af42f19ae84228e7b03cc7 |
| Source note | uspto-grants-1985_07 |