HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → 1H-Imidazole, 1-(1-naphthalenylmethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | 1H-Imidazole, 1-(1-naphthalenylmethyl)- | HCID 588244 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1H-Imidazole, 1-(1-naphthalenylmethyl)- | HCID 588244 | — |
| Product | Fumarate(1-) | HCID 6183479 | — |
Reaction Steps
A solution of fumaric acid (0.21 g) in hot ethanol (10 ml) was added to a solution of 1-(1-naphthylmethyl)imidazole (0.4 g) in ethanol (5 ml). After boiling for 10 minutes, the solution was evaporated under reduced pressure to afford a white solid. Recrystallisation of the solid from ethanol afforded 1-(1-naphthylmethyl)imidazole, hydrogen fumarate, m.p. 159°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04528195 |
| Source dataset | uspto-grants-1985_07 |
| ORD ID | ord-e1aa70e85ad849448a0703aeaf4bce23 |
| Source note | uspto-grants-1985_07 |